This paper has first summarized the experiment of granular film and theoretical research progress and the present major problem to be solved , has discussed the purpose meaning of this paper on this foundation , has introduced us soon afterwards with magnetic metal - non - magnetic metal material adopt for studying object to co - vapored deposited system such as the fexcu1 - x of different fe content x granular film sample , carrying out annealing handling for some of samples , using x ray diffraction instrument xrd ) , , scanning electrical microscopic ( sem ) , vibrating sample magnetometer ( vsm ) the tiny structure for sample , appearance and the magnetic result that can carry out detection 本文首先综述了颗粒膜的实验和理论研究进展情况和目前待解决的主要问题，在此基础上论述了本文的目的意义，随后介绍了我们以磁性金属?非磁性金属材料为研究对象，采用共蒸发法制备不同fe含量x的fe _ xcu _ ( 1 - x ) ，颗粒膜样品，对部分样品进行退火处理。给出了用x射线衍射仪( xrd ) 、扫描电镜( sem ) 、振动样品磁强计( vsm )对样品的微结构、形貌及磁性能进行检测的结果。
The microstructures and physics properties of the sbn films were characterized by xrd , afm , sims , raman scattering , and spectrophotometer , electrical induced birefringence etc . the effects of growth parameters on the quality of sbn films were discussed , such as substrates , annealing temperature , and precursor solution , bufferlayer ( ksbn , mgo ) 用x射线衍射仪( xrd ) 、原子力显微镜( afm ) 、二次离子质谱( sims ) 、受激拉曼散射、分光光度计、电致双折射(自建系统)等方法对sbn薄膜的结构性能和物理性能进行了表征。
By adopting x - ray diffraction and transmission electron microscope ( tem ) , this thesis has insepectd the size and the structure of the calcium carbonate ( caco3 ) particles . according to hydrophile and lipophile balance ( hlb ) , the suitable surface - active agents have been selected and put into lubricating oil with nanometer caco3 particles 本文采用x射线衍射仪和透射电镜检验了纳米碳酸钙粒子的粒径和内部结构，根据亲水亲油平衡值( hlb ) ，选择合适的表面活性剂将其加入到含有纳米碳酸钙粒子的润滑油中进行表面改性。
In this thesis , aragonite whisker was synthesized by introducing co2 into ca ( oh ) 2 suspension mixed with mgcl2 . the hyphenated technique of microscope - microcomputer was used to examine the morphology and microstructure of the products . the effects of reaction temperature , concentration of mgcl2 , ph value of the initial suspension , flow velocity of co2 , and stirring strength on the formation of the polymorphs of calcium carbonate were examined 本文利用改进的碳化法制备了文石相碳酸钙晶须，采用高倍显微镜一计算机联用技术、扫描电镜和x射线衍射仪进行产品形貌观察和晶型分析，讨论了温度、 mgcl _ 2浓度、初始ph值、 co _ 2的流速、搅拌速度等因素对制备文石相碳酸钙晶须的影响。
And then , zno thin films were synthesize on quartz and silicon substrates by sol - gel dip - coating and spin - coating . the properties of the films and the effects of growth parameters on the quality of zno films were studied using x - ray diffraction , optical absorption , photoluminescence techniques , etc . to modify the energy gap of the zno , mg2 + was added in the sol - gel solution , and mgxzn1 - xo films were prepared by the same method as that for zno films 利用溶胶凝胶法成功地在石英玻璃和单晶硅片等衬底上制备出了c轴择优取向的zno薄膜，并利用x射线衍射仪、紫外-可见光光谱仪、荧光光谱仪等对zno薄膜的结构和性能进行了测试、分析，并研究了热处理参数等条件对zno薄膜性能的影响。
